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Beilstein J. Org. Chem. 2010, 6, 932–937, doi:10.3762/bjoc.6.104
Graphical Abstract
Scheme 1: Preparation of the four [2.2]paracyclophane dialdehydes 4 by cycloaddition (ps - pseudo).
Scheme 2: Spin systems of the CH2CH2 protons in the isomeric dialdehydes 4. Protons at C-9 and C-10 in ps-gem...
Figure 1: CH2CH2 regions of the 600 MHz 1H NMR spectra of the isomeric dialdehydes 4, a: ps-gem, b: ps-meta, ...
Scheme 3: NOEs observed for ps-ortho-4 when the 5-H resonance is irradiated.